Standard Operating Procedures

Index No			Title
100			General and Corporate SOPs
101			CONTROL OF STANDARD OPERATING PROCEDURES AND TEST METHODS
110			ORGANIZATION AND FACILITIES
120			ROLES AND RESPONSIBILITIES
140			DOCUMENTATION OF TRAINING AND QUALIFICATIONS OF EMPLOYEES
170			SAMPLE AND WASTE DISPOSAL
190			COMPLAINT RESOLUTION
200			RADIATION SAFETY
210			HANDLING CONTROLLED SUBSTANCES
220			CHANGE CONTROL
240			HOUSEKEEPING, PEST CONTROL AND SECURITY
250			INTERNAL, THIRD PARTY AND VENDOR AUDITS
260			VENDOR QUALIFICATION
270			LABORATORY NON-CONFORMANCES, INCLUDING CORRECTIVE AND PREVENTATIVE ACTIONS
500			STUDIES PERFORMED UNDER GOOD LABORATORY PRACTICES (GLP) PROTOCOLS

900			Manuals
900			SAFETY MANUAL
930			QUALITY ASSURANCE MANUAL

1000			Clerical SOPs
1000			FILE STORAGE AND RETRIEVAL
1500			RECEIPT OF SAMPLES AND REVIEW OF CONTRACTS
1510			TEMPERATURE RECORDING AND REQUIRED LABELING FOR REFRIDGERATORS, FREEZERS, AND CONTROLLED TEMPERATURE AREAS MONITORING
1520			FOREIGN SOILS
1530			SAMPLE PRESERVATION CHECKING

2000			General Lab SOPs
2100			SOLUTIONS, REAGENTS, AND STANDARDS PREPARATION AND DOCUMENTATION
2110			CALIBRATION AND USE OF ANALYTICAL BALANCES
2120			DATA MANAGEMENT AND COMPUTING SYSTEMS
2130			NETWORK BACKUPS AND MAINTENANCE
2140			THERMOMETER CALIBRATION
2150			SUMMA CANISTERS
2160			LABORATORY DATA REVIEW AND GENERATION OF REPORTS
2170			CALIBRATION AND MAINTENANCE OF MECHANICAL PIPETTES
2180			DETECTION LIMITS
2190			SIGNIFICANT FIGURES AND ROUNDING
2200			WATER PURIFICATION
2220			METHOD VALIDATION
2230			OUT-OF-SPECIFICATION (OOS) INVESTIGATIONS
2240			GOOD DOCUMENTATION PRACTICES
2250			ANALYTICAL INSTRUMENT QUALIFICATION AND FACILITY EQUIPMENT MAINTENANCE
2260			CONTROL AND USE OF LABORATORY NOTEBOOKS, LOGBOOKS AND WORKSHEETS
2270			SOP FOR DATA ARCHIVE
2280			REAGENT CONTROL AND INVENTORY
2290			CALIBRATION AND USE OF pH METERS

2800			GLASSWARE CLEANING
2810			BNA EXTRACTIONS
2820			PESTICIDE EXTRACTION
2830			525 DRINKING WATER SAMPLE EXTRACTION
2840			PESTICIDE AND PCB CLEAN-UP

3000			Gas Chromatography
3000			VOLATILE ORGANICS IN DW BY EPA 502.2
3010			EDB & DBCP in DRINKING WATER
3020			NITROGEN AND PHOSPHORUS CONTAINING PESTICIDES
3030			HALOGENATED/AROMATIC VOLATILE ORGANICS
3040			HALOGENATED/AROMATIC VOLATILE ORGANICS
3050			FUEL HYDROCARBONS BY MODIFIED EPA 8015
3060			VOLATILE ORGANICS IN AMBIENT AIR.....
3070			VOLATILE HYDROCARBONS (C1-C9) AND PERMANENT GASSES...
3080			PHENOXY ACID HERBICIDES BY GC
3090			ORGANOCHLORINE PESTICIDES/PCBs BY GC
3100			ORGANOPHOSPHORUS PESTICIDES BY GC
3110			SILICONES
3120			GC MAINTENANCE
3130			INDUSTRIAL HYGIENE
3140			VOLATILE SULFUR
3150			ACRYLAMIDE IN POLYACRYLAMIDE POWDER BY GC/TSD
3160			EG AND ECH IN ALLERGAN AMO VITRAX
3170			ORGANIC VOLATILE IMPURITIES BY USP
3180			EG & ECH IN WATER
3190			ACETAMIDE BY GC
3200			BUTYLTIN
3210			DMSO - GC/FID
3220			ALCOHOL SCREEN
3230			BHT BY GC/FID
3240			ETO BY GC/FID HEADSPACE
3250			OVI IN *******
3260			ETHYLENE OXIDE, PROPYLENE OXIDE, AND 1,4-DIOXANE IN POLOXAMER
3270			RESIDUAL SOLVENTS IN PHOSPHOTIDYLCHOLINES BY GCFID
3280			FREE FATTY ACID METHYL ESTERS BY GCFID
3290			METHANE BY GC-FID (HEADSPACE)
3300			VOLATILE FUEL HYDROCARBONS
3310			9-ACETYLANTHRACENE PURITY BY GC/FID
3320			TOTAL IMPURITIES INCLUDING METHANOL IN METHYL FORMATE BY GC/FID
3330			ETHYLAMINE BY GC/FID
3340			HYDRAZINE BY GC
3350			DETERMINATION OF TRIBUTYL PHOSPHATE BY GC/TSD
3360			GC ANALYSIS FOR ORGANIC CONSTITUENTS

4000			Liquid and Ion Chromatography
4000			PNAs
4010			ALDEHYDES AND KETONES BY HPLC
4020			GENERAL ANIONS
4030			CARBAMATE-UREA PESTICIDES BY HPLC
4040			GENERAL CATIONS
4050			HEXAVALENT CHROMIUM BY EPA 218.6
4060			PHENOL AND CRESOLS BY EPA TO-8
4070			MOD. NIOSH 7600
4080			IC/LC MAINTENANCE
4090			MONOFLUOROPHOSPHATE IN TOOTHPASTE
4100			ANTIOXIDANTS BY HPLC
4110			GLYPHOSATE
4120			DIQUAT BY IC
4130			ORGANIC ANIONS
4140			HEXAVALENT CHROMIUM DIGESTION
4150			AZIDE
4170			PERCHLORATE BY IC
4190			Merit (IMIDACLOPRID)
4200			ACRYLAMIDE, ACRYLONITRILE, and ACROLEIN BY HPLC (EPA 8316)
4210			ASSAY OF SUCROSE BY IC
4220			ACETATE AND TRIFLUOROACETATE BY IC
4230			PHOSPHATE IN HYALURONDIDASE FORMULATIONS BY IC
4240			ASSAY OF LACTOSE IN HYALURONIDASE FORMULATIONS BY IC
4250			EDTA IN HYALURONIDASE FORMULATIONS BY HPLC
4260			ANALYSIS OF THIOLS BY PRECOLUMN DERIVATIZATION/HPLC
4270			BROMATE BY IC
4280			ANALYSIS OF TFA, ACETATE, AND FLUORIDE IN ******
4290			SODIUM DICHLOROACETATE BY IC
4300			BORATE BY IEC

5000			Mass Spectrometry
5000			SEMI-VOLATILE ORGANIC COMPOUNDS BY EPA 525
5010			SEMI-VOLATILE ORGANIC COMPOUNDS BY GCMS
5020			VOLATILE ORGANICS IN AIR BY GCMS
5030			GCMS SCREENS
5040			TCLP-ZHE LEACHATE PREPARATION..
5050			VOLATILE ORGANIC COMPOUNDS BY GCMS
5060			VOLATILE ORGANIC COMPOUNDS BY EPA 524.2
5070			TCLP SEMIVOLATILES
5080			USP 467 METHOD II
5090			PURGEABLE VOLATILE ORGANIC COMPOUNDS BY EPA METHODS 1666/524.2
5091			VOLATILE ORGANIC COMPOUNDS BY EPA METHOD 1666
5120			HP5973 GCMS MAINTENANCE
5130			ECH & EG IN NA HYALURONATE
5140			1,4-DIOXANE BY GCMS
5160			USP METHOD I & IV
5170			PNAs BY GCMS-SIM
5180			PESTICIDE SCREEN
5190			1,4-DIOXANE BY HEADSPACE GCMS
5200			QUALITATIVE DETERMINATION OF ADDITIVES IN METHYL METHACRYLATE
5210			DETERMINATION OF IMPURITES IN BONE BLACK
5220			DETERMINATION OF RESIDUAL SOLVENTS BY GCMS
5230			FURFURYL, FURFURAL, AND IPA BY GCMS
5240			ACRYLAMIDE BY ISOTOPE DILUTION GCMS
5250			MONOMERS
5260			ETHANEDITHIOL IN PROTEINS/PEPTIDES BY GCMS
5270			1,2,3-TRICHLOROPROPANE BY ISOTOPE DILUTION GCMS
5280			TRIETHYLAMINE BY GCMS

5510			PERCHLORATE BY LC-MS/MS
5520			p-CHLOROBENZENESULFONIC ACID (pCBSA) BY LC-MS/MS
5530			ARISTOLOCHIC ACID BY LC-MS/MS
5540			POLYSORBATE 80 BY LC-MS
5550			LOVASTATIN BY LC-MS/MS
5560			ALBUTEROL SULFATE BY LC-MS/MS
5570			MOLECULAR WEIGHT DETERMINATION BY ELECTROSPRAY MASS SPECTROMETRY

5900			CARBON, HYDROGEN AND NITROGEN BY COMBUSTION

6000			Spectroscopy
6000			CRYSTALLINE SILICA BY NIOSH 7602
6010			TOTAL HYDROCARBONS AND TOTAL PETROLEUM ....
6020			OIL & GREASE
6030			INFRARED SPECTROSCOPY
6040			OIL MIST-NIOSH
6050			IR MAINTENANCE
6500			NUCLEAR MAGNETIC RESONANCE

7000			Metals
7000			TOTAL BROMINE BY ICPMS
7020			MERCURY IN FISH
7030			TOTAL ORGANIC LEAD BY ICPMS
7040			TRACE METALS BY ICPMS
7050			URANIUM IN GROUNDWATER
7060			ALUMINUM IN PROTEIN
7070			PQ3 MAINTENANCE
7071			PQ4 MAINTENANCE
7080			SELECTED TRACE METALS IN POLY(DL-LACTIDE) POLYMER
7090			BORON BY ICPMS
7100			LI, AL, AND FE IN PEACH PEACH TWIG BORER (PTP) TECHNICAL
7110			IODINE IN PLASMA AND URINE
7120			HEAVY METALS
7130			LEAD IN ANTACIDS
7140			HYDRIDE ICPMS
7150			ELAN MAINTENANCE
7160			SILVER AND PALLADIUM IN ******* BY ICPMS
7170			SELECTED METALS IN SODIUM HYALURONATE
7180			SELECTED METALS IN LANTHANUM CARBONATE
7190			METALS BY ICP-OES
7210			TRACE METAL IMPURITIES IN SELENIUM DIOXIDE BY ICPMS
7220			TOTAL IRON CONTENT ASSAY IN ****** BY ICP-OES
7230			ARSENIC IN ********* BY ICPMS
7240			ARSENIC SPECIATION
7250			IODINE BY ICPMS
7260			LA IN SWABS BY ICPMS (FOSRENOL CLEANING VALIDATION)
7270			OPERATION OF AGILENT 7500CE ICPMS
7300			SILVER IN PLASMA BY ICPMS
7310			FREE GADOLENIUM SPECIATION IN GD-CHELATE AND DRUG PRODUCT BY LC/ICPMS
7320			SELECTED TRACE METALS IN EVAL POLYMERS
7330			SELENIUM IN WHOLE HUMAN BLOOD BY ICPMS
7340			DETEMINATION OF TIN IN LACTIDE/GLYCOLIDE COPOLYMERS

7500			OPERATION AND MAINTENANCE OF THE HYDRA AFG+ MERCURY ANALYZER

7600			METALS BY GFAA

7700			X-RAY FLUORESCENCE

7800			ACID DIGESTION OF SOILS....
7810			EP TOX LEACHATE...
7820			GLASSWARE CLEANING
7830			MICROWAVE DIGESTION
7840			TCLP LEACHATE PREPARATION.....
7850			WET LEACHATE PREPARATION....
7860			ACID DIGESTION OF FILTERS
7870			HIGH PURITY REAGENTS: OPERATION AND MAINTENANCE OF THE MILESTONE DUOPUR SUBBOILING DISTILLATION UNIT
7880			SAMPLE PREPARATION FOR ICPOES AND ICPMS ANALYSIS
7890			STANDARDS PREPARATION FOR ICPOES AND ICPMS ANALYSIS

8000			Wet Chemistry
8000			ACIDITY
8010			ALKALINITY
8020			AMMONIA BY NESSLERIZATION
8030			CHEMICAL OXYGEN DEMAND
8040			COLOR
8050			TOTAL AND AMENABLE CYANIDE
8060			DENSITY BY ASTM D1475
8070			FIXED AND VOLATILE SOLIDS
8080			FORMALDEHYDE BY NIOSH 3500
8090			HARDNESS
8100			WATER CONTENT BY KARL FISCHER TITRATION
8110			TOTAL MERCAPTANS IN WASTEWATER
8120			TOTAL PHENOLS
8121			TOTAL PHENOLS
8130			REACTIVE CYANIDES
8140			REACTIVE SULFIDES
8150			SALINITY
8160			SETTLEABLE SOLIDS
8170			pH OF SOIL AND WATER
8180			ELECTRICAL CONDUCTIVITY/SPECIFIC CONDUCTANCE
8190			SPOT TEST FOR CYANIDES IN CLEAN WATER
8200			SULFIDES IN SOILS AND WATERS
8210			SURFACTANTS (MBAS)
8220			TOTAL DISSOLVED SOLIDS
8230			TOTAL ORGANIC CARBON - WALKLY BLACK
8240			TOTAL SOLIDS
8250			TOTAL SUSPENDED SOLIDS
8260			TURBIDITY
8270			VOLATILE CONTENT
8280			FLASH POINT
8290			BIOLOGICAL OXYGEN DEMAND
8300			FLUORIDE BY ISE
8310			RESIDUAL CHLORINE
8320			SOLUBLE SULFIDE
8330			VITAMIN C ASSAY
8340			SCHIMADZU UV/VIS SPECTROPHOTOMETER
8350			BETA CAROTENE
8360			MELTING RANGE
8370			ORION 950 DISPENSER
8380			PHOSPHORUS SM45
8390			RESIDUE ON IGNITION
8400			LOSS ON DRYING
8410			IODINE TITRATION
8420			HEXAVALENT CHROMIUM BY COLORIMETRY
8430			ANALYSIS OF ******
8440			ASSAY OF t-BUTYLHYDROPEROXIDE
8450			GRAVIMETRIC ASSAY OF SELENIUM DIOXIDE
8460			DETERMINATION OF TWEEN-80 CONTENT
8470			HEM AND SGT-HEM EXTRACTION AND GRAVIMETRY BY EPA 1664

9000			STABILITY (Retired)